JAVELIN, GLADIUS, AND HASTA

Liquid Helium TEM Sample Holders

Based on our patented cooling principle, we offer cryo sample holders for different TEM brands. 

Liquid Helium TEM Sample Holders
Near absolute zero

Liquid Helium Temperatures

Our sample holders use liquid helium to reach a base temperature of 5.2 K. Starting from room temperature, the holder cools down to base within one minute, minimizing waiting time for measurements and optimizing microscope use. Once cold, this temperature can be held with a temperature stability of +/- 2.5 mK for as long as there is helium in the dewar, which can easily exceed 24 hours. We currently offer holders that are compatible with JEOL, Thermo Fischer Scientific, and Nion electron microscopes. For maximum resolution, these sample holders are used in conjunction with our CORVUS cryogenic stage and the TUBUS liquid helium transfer line. 

GLADIUS TFS-Compatible Sample Holder
Navigating phase diagrams

In-Situ Capabilites

Samples, mounted onto standard 3 mm TEM grids, can be fixed onto a chip which easily slides into the sample holder. Each sample holder can be upgraded with optional electrical contacts — established via a set of pogo pins —  to enable electrical biasing. We are currently working on developing MEMS chips to provide localized sample heating for measurements from liquid helium temperature up to room temperature. 

 

Sample Holder with Radiation Shield and Chip Removed

 

Close-up of Sample Holder

 

Sample Holder with Radiation Shield Removed

 

Radiation Shield Removed and Chip Receiver Opened

 

TEM Chip Slides Out of Holder

 

Under Development

Cryo-Cathodoluminescence

Our team is in the process of engineering a specialised liquid helium holder, tailored specifically for use with NION transmission electron microscopes. In addition to its primary function, this innovative holder can be modified to facilitate cathodoluminescence (CL) experiments, particularly catering to the needs of the Research Group LPS led by Dr. Mathieu Kociak at the University of Paris-Sud. For the CL setup, we utilise the Mönch light-collecting mirror, which is positioned from the side and supplied by Attolight. This project marks the debut of a NION-compatible sample holder designed by condenZero, with the installations scheduled for completion by 2025.

HASTA Cathode Luminescence Holder